Contents
Journal of Analitical Chemistry

Vol. 58, No. 7, 2003

Simultaneous English language translation of the journal is available from MAIK “Nauka / Interperiodica” (Russia).
Distributed worldwide by Kluwer Academic / Plenum Publishers. Journal of Analytical Chemistry ISSN 1061-9348.

From the Editor-in-Chief

2002 Nobel Prize Awarded for the Development of Analytical Methods p. 609

Abstracts of Papers of the International Symposium
“Separation and Preconcentration in Analytical Chemistry”
Devoted to the 70th Birthday of Academician Yu. A. Zolotov

From the Editorial Board of Zhurnal Analiticheskoi Khimii p. 610

Metrological Aspects of Separation and Preconcentration in Chemical Analysis

Yu. A. Karpov p. 610

Dynamic Sorption Preconcentration of Compounds in Analytical Chemistry

G. I. Tsizin and Yu. A. Zolotov p. 611

Chemically Modified Complexing Silicas: Predicting Analytical Applications

V. N. Zaitsev p. 612

Modified Silicas: Preconcentration, Separation, and Determination
of Inorganic and Organic Compounds

E. I. Morosanova p. 612

Study of the Sorption Properties of Cellulose Acetate Modified
with Aluminon and Eriochrome Cyanine R

S. A. Akhmedov, M. P. Kazalieva, M. S. Spirina, and N. A. Adakova p. 613

Preconcentration of Organic Compounds on Foamed Polyurethanes:
Regularities and Examples of Analytical Application

S. G. Dmitrienko, L. N. Pyatkova, O. M. Medvedeva, and Yu. A. Zolotov p. 614

Sorptive Extraction of Gold(III) with Silica Gels Chemically Modified
with Mercapto, Amino, and Disulfide Groups

V. N. Losev, E. V. Buiko, E. V. Elsuf’ev, A. K. Trofimchuk, E. B. Andrianova, and A. V. Legenchuk p. 614

Fibrous Filled Sorbents: Possibilities and Potentialities
in the Preconcentration and Separation of Elements

G. V. Myasoedova, E. A. Zaharchenko, and V. A. Nikashina p. 615

Preconcentration and Determination of Palladium Using Silica Gels Chemically
Modified with Mercapto and Disulfide Groups

V. N. Losev, Yu. V. Kudrina, and A. K. Trofimchuk p. 616

Sorption of Transition Metals on Monolith CIM Discs Modified
with Oligoethyleneamines

M. A. Rybalko and P. N. Nesterenko p. 616

Study of the Effect of the “Third” Component on the Sorption of Elements
in the System Chelating Sorbent–Element–para-Substituted Anilines

N. N. Basargin, I. M. Kutyrev, Yu. A. Chebotnikova, V. A. Golosnitskaya,
M. N. Astakhova, and Yu. G. Rozovskii p. 617

Preconcentration and Determination of Traces of Heavy Metals
with Polymer Chelating Sorbents in the Analysis of Natural and Waste Water

N. N. Basargin, E. R. Oskotskaya, G. I. Karpushina, V. G. Senchakov, and Yu. G. Rozovskii p. 617

Physicochemical Conditions of the Sorption of Copper(II) Ions
with a Polymer Chelating Sorbent Based on N-Aryl-3-Aminopropionic Acids

L. K. Neudachina, A. A. Vshivkov, Yu. A. Skorik, Yu. G. Yatluk, and Ya. A. Kukushkina p. 618

Atomic Absorption Determination of the Dissolved and Suspended Forms
of Elements in Natural Water with Dynamic Sorption Preconcentration in Atomizers

V. N. Oreshkin, G. I. Tsizin, and Yu. A. Zolotov p. 619

A New Device for On-Line Dynamic Sorption Preconcentration

V. A. Pribytkov and E. M. Rukin p. 619

Thin-Layer Cellulose Filters for the Preconcentration of Elements from Solutions

G. I. Tsizin, V. P. Gordeeva, A. A. Formanovskii, I. V. Mikhura, and Yu. A. Zolotov p. 620

Reactive–Adsorptive Preconcentration on Smooth Surfaces

V. V. Yagov p. 620

Chemisorption Preconcentration of Nonmetals and Organic Compounds
on Polyurethane Foams for Their Determination by Diffuse Reflectance Spectroscopy

L. N. Pyatkova, S. G. Dmitrienko, O. A. Sviridova, S. A. Badakova, and Yu. A. Zolotov p. 621

Electrothermal Atomic Absorption Determination of Trace Lead and Cadmium
in Urine after Preconcentration and Separation from the Matrix on a DETATA Adsorbent

I. L. Grinshtein, L. A. Vasil’eva, and Yu. V. Maksimova p. 622

Sorption of Anionic Metal Complexes and Color Reactions with Organic Reagents
on the Solid Phase of a Fibrous Filled Sorbent

V. P. Dedkova, O. P. Shvoeva, and S. B. Savvin p. 622

Sorption and Determination of Vanadium(IV, V) and Mercury(I, II)
as Their Colored Complexes of Organic Reagents

R. F. Gur’eva, S. B. Savvin, and A. V. Mikhailova p. 623

Adsorption–Catalytic Determination of Metal Inhibitors

E. N. Kiryushchenkov, T. A. Stoyan, M. K. Beklemishev, and I. F. Dolmanova p. 624

Preconcentration and Separation of Components in Adsorption–Catalytic Analysis

T. N. Shekhovtsova, I. F. Dolmanova, and M. K. Beklemishev p. 625

Flow Sorption Preconcentration in the Determination of Phenols
by Reversed-Phase High-Performance Liquid Chromatography

O. A. Filippov, T. I. Tikhomirova, E. N. Shapovalova,
G. I. Tsizin, O. A. Shpigun, and Yu. A. Zolotov p. 625

Continuous Adsorption Sampling in Industrial Monitoring of the Dust
and Gas Content in the Air of a Working Area and Process Gas Emissions

Z. L. Baskin p. 626

Coordination Chemistry in Analytical Methods Separation of Element Mixtures

O. M. Petrukhin p. 626

Hydration–Solvation Mechanism in Micellar Extraction

R. K. Chernova p. 628

Optimization of the Photometric Determination of Aromatic Amines
with Preconcentration in a Micellar Phase of Anionic Surfactants

N. N. Gusakova and R. K. Chernova p. 628

A Method of Flow Solvent Extraction from Solid Substances

N. A. Klyuev, A. A. Shelepchikov, V. S. Soifer, and E. S. Brodskii p. 629

Extraction Preconcentration of Hydrophobic and Hydrophilic Binuclear Aromatic Compounds

Ya. I. Korenman, P. T. Sukhanov, and S. P. Kalinkina p. 630

Hydrophilic Phases in the Solvent Extraction of Organic Compounds

Ya. I. Korenman and T. A. Kuchmenko p. 631

Flow Extraction Preconcentration: Extraction–Chromatographic Extraction
with the Chromatomembrane Separation of the Extract from the Aqueous Phase

A. L. Moskvin and E. A. Mukhina p. 632

Ionic Liquids as New Solvents for Extraction and Analysis

I. V. Pletnev, A. A. Formanovskii, S. V. Smirnova, I. I. Torocheshnikova,
K. S. Khachatryan, N. V. Shvedene, and M. Yu. Nemilova p. 632

Screening for Psychotropic Drugs in Human Hair Based on a Combination
of Microliquid Extraction and High-Performance Thin-Layer Chromatography

T. V. Polenova, I. V. Marutsenko, A. G. Borzenko, and I. A. Revel’skii p. 633

Hyphenated Extraction– and Membrane–Electrochemical Methods
for Determining Elements with the Use of Water-Soluble Polymers

V. M. Shkinev and E. A. Osipova p. 633

Comparison of the Direct-Flow and Counterflow Techniques of Chromatomembrane
Gas Extraction in the Determination of Alkyl Acetates in Aqueous Solutions

O. V. Rodinkov and N. A. Maiorova p. 634

Determination of Chlorophenols in Potable Water: Preconcentration
by Solvent Extraction, Derivatization of the Extract,
and Chromatographic Analysis of the Derivatives

Ya. I. Korenman, I. V. Gruzdev, B. M. Kondratenok, and V. N. Fokin p. 635

Micellar Extraction as a Method to Control Analytical Reactions

R. K. Chernova, S. Yu. Doronin, L. M. Kozlova, A. N. Pankratov, and O. I. Zhelezko p. 636

New Hyphenated Method for the Preconcentration and Extraction of Arsenic
for Its Flow-Injection Determination

L. N. Moskvin, A. V. Bulatov, G. L. Grigor’ev, and G. I. Koldobskii p. 637

Use of Preconcentration for Sample Preparation in X-ray Fluorescence Analysis

E. N. Maiorova p. 637

Separation and Preconcentration in Neutron Activation Analysis

G. G. Glukhov p. 638

Fire-Assay as a Method for the Preconcentration of Noble Metals

G. M. Kolesov and D. Yu. Sapozhnikov p. 638

Immunoextraction of Pesticide Residues from Different Classes Followed
by Amperometric Determination

E. P. Medyantseva, N. Yu. Il’icheva, S. A. Eremin, and G. K. Budnikov p. 639

High-Performance Planar Chromatography

V. D. Krasikov and I. I. Malakhova p. 640

Use of Sulfonated Hypercross-Linked Polystyrene in Ion Chromatography

P. A. Kebets and P. N. Nesterenko p. 641

Determination of the Nitrite Ion by Ion Chromatography with Catalytic Detection

M. A. Dikunets, A. I. Elefterov, and O. A. Shpigun p. 641

Determination of Food Dyes by Thin-Layer Chromatography with Cyclodextrin Mobile Phases

V. Z. Atayan, E. G. Sumina, and S. N. Shtykov p. 642

Preconcentration of Impurities in Ethanol with the Use of Rayleigh Distillation

V. A. Krylov, A. V. Mitin, and O. Yu. Chernova p. 642

Procedure for the TLC Screening of Biological Objects Based
on the Relative Migration Times of the Components

Z. A. Temerdashev, N. V. Kiseleva, A. V. Udalov, and R. A. Klishchenko p. 643

Increasing the Information Content of the GLC Screening of Narcotic and Potent Preparations
with the Use of a Multidetector

A. V. Udalov, V. V. Kolesnikov, and L. D. Karaeva p. 643

Hydrolytically Stable Zirconyl-Containing Microspherical Silica Gels
for High-Performance Liquid Chromatography

S. Sh. Rashidova, S. V. Zalyalieva, O. A. Shpigun, V. D. Krasikov, and B. D. Kabulov p. 644

Determination of Individual Species by Liquid Chromatography Combined
with an Element-Selective Detector Based on Diode Laser Atomic Absorption Spectrometry

M. A. Bol’shov, A. V. Zybin, D. Butcher, and K. Niemax p. 645

Some Problems in the Theory of Adsorption–Catalytic Stripping Voltammetry

O. E. Ruvinskii, N. S. Abramova, and V. N. Sirko p. 646

Preconcentration in the Electrode Bulk: New Potentialities
in the Development of Voltammetry

V. N. Maistrenko and G. K. Budnikov p. 647

Voltammetric Determination of Sulfhydryl Compounds
with Preconcentration at a Mercury Film Electrode

E. Sh. Alieva, T. G. Tsyupko, and Z. A. Temerdashev p. 648

Analytical Potentialities of Amperometric Detection in HPLC

Ya. I. Yashin and A. Ya. Yashin p. 649

Determination of Amino Acids by Capillary Electrophoresis
without Preliminary Derivatization

A. V. Shpak, A. V. Pirogov, and O. A. Shpigun p. 649

Electrophoresis and Electrochromatography with Polycapillary Columns

V. V. Nikonorov p. 650

Separation of Heavy Metal Cations in Electrophoretically Mediated Microanalysis

O. I. Markova, T. G. Nikitina, A. A. Krasheninnikov, and V. P. Andreev p. 650

Preconcentration of Heavy Metals on Immobilized Deoxyribonucleic Acid
Incorporated into a Biosensor for Determining Metals in Biological Samples

S. S. Babkina, N. A. Ulakhovich, E. N. Moiseeva, and E. E. Filyushina p. 651

Preconcentration of Exhaust Gas Followed by the Determination of Heavy Metal Cations
and Acid-Forming Oxides in a Multisensor Flow-Injection System

A. V. Ipatov, A. V. Legin, and Yu. G. Vlasov p. 652

Micelles and Microemulsions in Separation and Preconcentration

S. N. Shtykov, I. Yu. Goryacheva, and L. S. Shtykova p. 652

Fractionation of Solid Particles Present in Water in Rotating Coiled Columns

O. N. Katasonova, P. S. Fedotov, V. A. Kronrod, and B. Ya. Spivakov p. 653

Preconcentration of Anionic Metal Complexes with Hydrophilic Surfactants
on Liquid Spherical Membranes and Inverted Micelles

A. I. Bulavchenko, T. Yu. Podlipskaya, E. K. Batishcheva, T. L. Popova, and V. G. Torgov p. 654

Separation of Anionic, Cationic, and Nonionic Surfactants
in Homologous Series Using Molecular Sieves

E. G. Kulapina, R. K. Chernova, A. I. Kulapin, S. A. Mitrokhina, N. M. Mikhaleva, and V. V. Kurina p. 655

Preconcentration of Impurities by Matrix Elimination in the Analysis
of High-Purity Substances by Atomic Emission and Atomic Absorption Spectrometry

V. G. Pimenov p. 656

New Developments in Element Preconcentration by Sample Matrix Distillation

I. R. Shelpakova, L. N. Komissarova, N. P. Zaksas, S. V. Kovalevskii, and A. I. Saprykin p. 656

Fractional Evaporation as a Method for Trace Element Preconcentration
in the Analysis of Rocks and Minerals

V. P. Bukar’ p. 657

Separation and Preconcentration in Flow-Injection Analysis

L. K. Shpigun p. 658

Potentialities of the Analytical Crystallization Preconcentration of Impurities in Solutions

L. P. Eksperiandova and A. B. Blank p. 658

Test Methods for Determining Zinc(II) and Lead(II) Using Immobilized
Alkaline Phosphatases of Different Origin

I. A. Veselova, A. M. Zhavoronkova, S. V. Muginova, and T. N. Shekhovtsova p. 659

A Test Method for Determining Active Chlorine in Drinking Water

M. O. Gorbunova and I. N. Zhikhareva p. 660

Reliable Estimation of the Limit of Detection in Test Methods with Visual Indication

E. A. Reshetnyak and Yu. V. Kholin p. 660

Microfluidic Analysis Systems

V. E. Kurochkin and A. A. Evstrapov p. 661

Sorption–Catalytic Determination of Polymers

A. L. Kapanadze, M. K. Beklemishev, O. M. Abramova,
T. D. Gushchina, and I. F. Dolmanova p. 662

Chromatomembrane Generation of Standard Gas Mixtures Containing
Atmospheric Pollutants at a Level of g/L

L. N. Moskvin and T. G. Nikitina p. 662

Preconcentration in the Analysis of High-Purity Volatiles

V. A. Krylov p. 663

Separation of -Blockers on Chiral Stationary Phases Based
on the Teicoplanin Macrocyclic Antibiotic

I. A. Anan’eva, E. N. Shapovalova, O. A. Shpigun, and D. W. Armstrong p. 663

Articles

Estimation of the Sampling Error in the Determination of Benzo[a]pyrene
in Organized Gas–Dust Air Emissions

L. I. Belykh, Yu. M. Malykh, A. N. Smagunova, E. E. Penzina, and V. A. Kozlov p. 665  abstract

Formation and Role of a Hollow-Cathode Plasma Plug in Mass-Spectrometric Analysis

G. G. Sikharulidze and A. E. Lezhnev p. 673  abstract

Determination of Vanillin and Ethylvanillin in Vanilla Flavorings
by Planar (Thin-Layer) Chromatography

A. V. Gerasimov, N. V. Gornova, and N. V. Rudometova p. 677  abstract

Optimization of Conditions for the HPLC Determination of Synthetic Dyes in Food

M. G. Kiseleva, V. V. Pimenova, and K. I. Eller p. 685  abstract

A Zinc-Selective Electrode with a Low Detection Limit
and Its Use in the Analysis of Environmental Samples

E. M. Rakhman’ko, V. V. Egorov, M. Ya. Tarazevich, and A. D. Rubinova p. 691  abstract

Chronicle

International Symposium on Separation and Preconcentration in Analytical Chemistry p. 698

The 75th Birthday of A. N. Mogilevskii p. 699

Instructions for Authors p. 701

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