Radial Dependences of the Phase Composition, Nanohardness, and Young’s Modulus for Ti–2 wt % Fe Alloy after High-Pressure Torsion
A. S. Gornakovaa, *, S. I. Prokofjeva, N. S. Afonikovaa, A. I. Tyurinb, A. R. Kilmametovc, A. V. Kornevad, and B. B. Straumala
aOsipyan Institute of Solid State Physics, Russian Academy of Sciences, Chernogolovka, 142432 Russia
bResearch Institute of Nanotechnology and Nanomaterials, Derzhavin Tambov State University, Tambov, 392000 Russia
cProcess and Materials Science Laboratory, Sorbonne Paris Nord University, Villetaneuse, 93430 France
dAleksander Krupkowski Institute of Metallurgy and Materials Science, Polish Academy of Sciences, Krakow, 30059 Poland
email: *alenahas@issp.ac.ru
Received 25 January, 2024
Abstract— The specimens of Ti–2 wt % Fe alloy were annealed at three different temperatures, in the β-Ti, α-Ti + β-Ti and α-Ti + TiFe fields of the Ti–Fe phase diagram, then water quenched and subjected to high-pressure torsion (HPT). The X-ray diffraction analysis showed that the main phase in all annealed specimens was the α phase (more than 90%), while the main phase after HPT was the ω phase. Hardness H and Young’s modulus E were determined by nanoindentation at the center, in the middle of the radius, and near the edge of each specimen. It was found that the H and E values were different for specimens annealed at different temperatures and depended on the radial coordinate of the indentation region. The maximum H values were obtained in the middle of the radius of the specimens. The E values of all specimens decreased from the center to the edge, reaching very low values. The paper discusses structure transformations during HPT, the behavior of the radial dependences of H and E, and probable causes of a strong decrease in E values.
Keywords:
titanium alloys,
high-pressure torsion,
nanoindentation,
hardness,
Young’s modulus,
phase transformations,
influence of the initial microstructure
DOI: 10.1134/S1029959924060018