Glycineframe0Nitrate Combustion Synthesis of Finely Dispersed
Alumina

V. D. Zhuravleva,*, V. G. Vasil’eva, E. V. Vladimirovaa, V. G. Shevchenkoa,
I. G. Grigorov
a, V. G. Bamburova, A. R. Beketovb, and M. V. Baranovb

aInstitute of Solid State Chemistry, Ural Branch, Russian Academy of Sciences,
ul. Pervomaiskaya 91, Yekaterinburg GSP-145, 620990 Russia

*e-mail: zhvd@ihim.uran.ru

bB. N. Eltsyn Ural State Technical University (UPI), ul. Mira 21, Yekaterinburg, 620002 Russia

Received October 6, 2009

Abstract—The possibility of synthesizing different crystalline modifications of alumina Al2O3 by combustion
reactions of a mixture of aluminum nitrate with glycine has been analyzed. Aggregated powders of -Al2O3 that
do not transform into the corundum structure after annealing at a temperature of 1000C have been prepared.
The influence of the synthesis conditions on the specific surface area, bulk density, porosity, and morphology
of alumina particles has been investigated.

Key words: combustion reactions, alumina, glycine–aluminum nitrate mixtures, combustion synthesis, ther-
molysis, crystallites, nanopowders

DOI: 10.1134/S1087659610040164


Pleiades Publishing home page | journal home page | top

If you have any problems with this server, contact webmaster.