Fabrication, Morphological, and Thermal Investigation of Epoxy-Polyamide Nanocomposites Reinforced with Carbon Nanotubes
Song Wanga,*, Bahar Alib, Mehwish Javedb, Sahid Mehmoodb, Farman Alib,**, Zarshad Alib,
Siddiqa Begumb, Nisar Alia,***, Naseer Iqbalc, and Muhammad Sajidd
a National and Local Joint Engineering Research Center for Mineral Salt Deep Utilization,
Huaiyin Institute of Technology, Huaian, 223003 China
b Department of Chemistry, Hazara University, Mansehra KPK, 21300 Pakistan
c College of Science, University of Hafr Al Batin, Al Jamiah, Hafar Al Batin, 39524 Saudi Arabia
d School of Life Science and Food Engineering, Huaiyin Institute of Technology, Huaian, 223003 China
Correspondence to: * e-mail: wangsong@hyit.edu.cn
Correspondence to: ** e-mail: farmanqau@gmail.com
Correspondence to: *** e-mail: nisarali@hyit.edu.cn
Received 27 April, 2023
Abstract—Epoxy-polyamide CNTs reinforced nanocomposites have the excessive ability for their uniform structures and specific properties and have considerable attention owing to their potential applications. In this work, epoxy/polyamide (ER-PA) and CNTs reinforced epoxy/polyamide (ER-PA/CNTs) nanocomposites were prepared by using the solution casting method. Herein, Fourier transforms infrared spectroscopy (FT-IR) was applied to indicate the responsible functional groups, presented in the prepared nanocomposites. Surface morphology and particle dispersion of the prepared nanocomposites were examined by scanning electron microscopy (SEM). The obtained results demonstrated that the CNT’s weight content, dispersion rates, and the surface functionalization of CNTs nanoparticles have a strong influence on the surface morphology of the prepared nanocomposites. The thermal properties and crystalline nature of the ER-PA/CNTs nanocomposites were studied by using thermogravimetric analysis (TGA) and X-ray diffraction (XRD) analyses. The prepared nanocomposites showed good thermal stability and crystalline behavior as compared to the ER-PA nanocomposites network system. From the obtained results, it can be assumed that this effort can help to design other reinforced nanocomposites for promising applications in the nanocomposites materials industry.
Abstract—
Keywords: epoxy resin, polyamide, carbon nanotubes, reinforced, nanocomposites, morphology, thermal properties
DOI: 10.1134/S0036024423130289