Synthesis and Analysis of the Indium–Gallium–Zinc Oxide Semiconductor Structure
D.A.Vinnika, b, c, A.I.Kovaleva, *, D.P.Sherstyuka, D.E.Zhivulina, G.M.Zirnikb, and T.V.Batmanovad
aSouth Ural State University (National Research University), Chelyabinsk, Russia
bMoscow Institute of Physics and Technology, Dolgoprudny, Russia
cSt. Petersburg University, St. Petersburg, Russia
dChelyabinsk State University, Chelyabinsk, Russia
email: *kovalev-andrey-i@mail.ru
Received 30 September, 2024
Abstract— A solid-phase synthesis of the InGaZn
2O
5 semiconductor oxide is reported; its phase composition, structure, and morphology are analyzed using XRD, full-profile XRD analysis, scanning electron microscopy, energy-dispersive X-ray spectroscopy, IR spectroscopy, and Raman spectroscopy. It is shown that the studied compound corresponds to the InGaZn
2O
5 structure,
P6
3/
mmc space group; its structural parameters are reported. The sample prepared under the chosen conditions has morphology characterized by polydispersity, presence of agglomerates, and by the absence of pronounced crystallite faceting. IR and Raman spectra of InGaZn
2O
5 are reported for the first time.

Keywords: IGZO, indium–gallium–zinc oxide, solid-phase synthesis, SEM, EDX, XRD, IR spectroscopy, Raman spectroscopy.
DOI: 10.1134/S0022476625020052