X-ray Diffraction Method for the Determination
of Residual Internal Stresses in Cement

E. D. Shchukin*, L. M. Rybakova**, L. I. Kuksenova**, and E. A. Amelina*

* Department of Chemistry, Moscow State University, Vorob’evy gory, Moscow, 117234 Russia
** Blagonravov Institute of Mechanical Engineering, Russian Academy of Sciences,
M. Khariton’evskii per. 4, Moscow, 101830 Russia

Received June 25, 1996

Abstract—A new X-ray diffraction technique is developed, for the first time enabling the detection of internal
microstresses (of the II mode) developing in cement hardening structures in the course of their formation, and
macrostresses (of the I mode) caused by capillary forces during the removal of pore-confined water. Prospects
of the application of this method are demonstrated for estimating the effect of various factors on the quality of
cement materials.


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